Propylethinylcarbinol → 3-(2-Ethoxyethoxy)-1-hexyne

HRID 1080887

반응식

[CH:1]#[C:2][CH:3]([OH:7])[CH2:4][CH2:5][CH3:6].[CH2:8]([O:10][CH2:11][CH2:12]Br)[CH3:9]>>[CH2:8]([O:10][CH2:11][CH2:12][O:7][CH:3]([CH2:4][CH2:5][CH3:6])[C:2]#[CH:1])[CH3:9]

참가 물질

반응물 2

HCID 7746Propylethinylcarbinol

HCID 611412-Bromoethyl ethyl ether

생성물 1

HCID 233661663-(2-Ethoxyethoxy)-1-hexyne수율 44.7%

실험 절차

In accordance with the procedure of the step 1 of Example 10, 21.8 g of 1-hexyn-3-ol was allowed to react with 37.2 g of 2-bromoethyl ethyl ether to obtain 16.9 g of 3-(2-ethoxyethoxy)-1-hexyne.

출처 및 근거

ORD 기록: ord-3620d65f5beb4852ba49c5544d4dd0c7
출처 데이터셋: uspto-grants-1996_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05583227

연결된 노트

불러오는 중…