2,4-Diamino-5-(2,3-dichlorophenyl)-6-methylpyrimidine → 2,4-Diamino-5-(2,3-dichloro-4-nitrophenyl)-6-methylpyrimidine

HRID 1081590노트

반응식

HRID 1081590 반응식
[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[C:11]([Cl:15])[C:10]=2[Cl:16])=[C:4]([CH3:17])[N:3]=1.NC1C=C(N)C(C2C=CC([N+:32]([O-:34])=[O:33])=CC=2C2C=CC=C(Cl)C=2Cl)=CN=1.NC1N=C(N)C(C2C=C([N+]([O-])=O)C=C(Cl)C=2Cl)=C(C)N=1>>[NH2:1][C:2]1[N:7]=[C:6]([NH2:8])[C:5]([C:9]2[CH:14]=[CH:13][C:12]([N+:32]([O-:34])=[O:33])=[C:11]([Cl:15])[C:10]=2[Cl:16])=[C:4]([CH3:17])[N:3]=1

참가 물질

4

반응물 3

HCID 116734192,4-Diamino-5-(2,3-dichlorophenyl)-6-methylpyrimidineHCID 197051082,4-Diamino-5(2,3-dichloro-5-nitrophenyl)-6-methylpyrimidineHCID 233628052,4-Diamino-5-(2,3-dichlorophenyl-4-nitrophenyl)pyridine

생성물 1

HCID 197050312,4-Diamino-5-(2,3-dichloro-4-nitrophenyl)-6-methylpyrimidine

실험 절차

This compound was made from the compound of Example 15 in an analogous manner to the compound of Example 39, mp. 265° C. Also obtained from this reaction was 2,4-diamino-5(2,3-dichloro-5-nitrophenyl)-6-methyl pyrimidine.

후처리

  1. customAlso obtained from this reaction

출처 및 근거

ORD 기록
ord-8f2bc6d903b84ba5a451356374fac1a3
출처 데이터셋
uspto-grants-1996_12
특허 번호
US05587380

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