Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5,6-Diamino-1,3-dimethyluracil → 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxy-3-methylphenyl)ethenyl)-1,3-dimethyl-, (E)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5,6-Diamino-1,3-dimethyluracil | HCID 79501 | — |
| 반응물 | 2,4-Dimethoxy-3-methylcinnamic acid | HCID 53401577 | — |
| 생성물 | 1H-Purine-2,6-dione, 3,7-dihydro-8-(2-(2,4-dimethoxy-3-methylphenyl)ethenyl)-1,3-dimethyl-, (E)- | HCID 6448870 | 28% |
반응 단계
Substantially the same procedure as in Example 7 was repeated using 1.0 g (5.88 mmol) of 5,6-diamino-1,3-dimethyluracil and 1.44 g (6.45 mmol) of 2,4-dimethoxy-3-methylcinnamic acid. Then, the resultant crude crystals were recrystallized from dioxane to give 581 mg (yield 28%) of Compound 94 as pale yellow needles.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05587378 |
| 출처 데이터셋 | uspto-grants-1996_12 |
| ORD ID | ord-de9f240a3b6546b7a1e8395f3b20dcd3 |
| 출처 메모 | uspto-grants-1996_12 |