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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1081792생성일: 2026년 10월 27일

3-(2,3,4-Trimethoxyphenyl)-2-propenoic acid → 1H-Purine-2,6-dione, 3,7-dihydro-1,3-dipropyl-8-(2-(2,3,4-trimethoxyphenyl)ethenyl)-, (E)-

https://huagongshe.com/reaction/1081792

반응식

참여 물질

역할이름HCID투입량
반응물3-(2,3,4-Trimethoxyphenyl)-2-propenoic acidHCID 118400—
반응물5,6-Diamino-1,3-dipropyl-2,4(1H,3H)-pyrimidinedioneHCID 5098605—
생성물1H-Purine-2,6-dione, 3,7-dihydro-1,3-dipropyl-8-(2-(2,3,4-trimethoxyphenyl)ethenyl)-, (E)-HCID 644875749%

반응 단계

Substantially the same procedure as in Reference Example 1 was repeated using 2.00 g (8.85 mmol) of 5,6-diamino-1,3-dipropyluracil and 2.32 g (.9.73 mmol) of 2,3,4-trimethoxycinnamic acid. Then, the resultant crude crystals were recrystallized from 2-propanol/water to give 1.84 g (yield 49%) of Compound 20 as pale yellow needles.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05587378
출처 데이터셋uspto-grants-1996_12
ORD IDord-ab16c08a572541da81bddf1c78daa415
출처 메모uspto-grants-1996_12