Benzoic Acid → Benzoic acid--piperidine (1/1)

HRID 1084463노트

반응식

HRID 1084463 반응식
[C:1]([OH:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH:10]1[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1>CC(C)=O>[NH:10]1[CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1.[C:1]([OH:9])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 243Benzoic AcidHCID 8082Piperidine

생성물 1

HCID 6452737Benzoic acid--piperidine (1/1)수율 89.9%

시약·촉매·용매 1

HCID 180Acetone용매

실험 절차

To a solution of 12.2 g (0.1 mol) of benzoic acid dissolved in 100 ml of acetone, 8.5 g (0.1 mol) of piperidine was added dropwise. The crystals precipitated were filtered, and then dried, and benzoic acid piperidine salt (molar ratio 1:1) of white crystals was obtained in an amount of 18.6 g (yield 89.9%).

후처리

  1. customThe crystals precipitated
  2. filtrationwere filtered
  3. customdried

출처 및 근거

ORD 기록
ord-9dc375534956400f9ddc4fd5a05d807b
출처 데이터셋
uspto-grants-1991_04
특허 번호
US05004787

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