Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → Diethyl 3-phenyl-2-isoxazolin-5-ylmethylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | (Z)-Benzaldehyde oxime | HCID 12143 | — |
| 반응물 | Chlorosuccinimide | HCID 31398 | — |
| 반응물 | Diethyl allylphosphonate | HCID 573014 | — |
| 생성물 | Diethyl 3-phenyl-2-isoxazolin-5-ylmethylphosphonate | HCID 20062399 | — |
반응 단계
In analogy to Example 1, 76.7 g of an oily crude product are obtained starting from 30.3 g (0.25 mol) of benzaldoxime, 36.7 g (0.275 mol) of N-chlorosuccinimide, 49 g (0.275 mol) of diethyl allylphosphonate and 38.2 ml (0.275 mol) of triethylamine and can be purified as described in Example 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05006515 |
| 출처 데이터셋 | uspto-grants-1991_04 |
| ORD ID | ord-9ec388885fd14ede8f3fc57e3c0d5276 |
| 출처 메모 | uspto-grants-1991_04 |