Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → Dimethyl 3-(3-phenoxyphenyl}-2-isoxazolin-5-ylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Chlorosuccinimide | HCID 31398 | — |
| 반응물 | Dimethyl vinylphosphonate | HCID 78376 | — |
| 반응물 | N-[(3-phenoxyphenyl)methylidene]hydroxylamine | HCID 2393595 | — |
| 생성물 | Dimethyl 3-(3-phenoxyphenyl}-2-isoxazolin-5-ylphosphonate | HCID 20062400 | 95.6% |
반응 단계
In analogy to Example 1, 42.65 g (0.2 mol) of 3-phenoxybenzaldoxime, 29.4 g (0.22 mol) of N-chlorosuccinimide, 29.2 ml (0.22 mol) of dimethyl vinylphosphonate and 30.6 ml (0.22 mol) of triethylamine are reacted, and 66.4 g of oily product are obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05006515 |
| 출처 데이터셋 | uspto-grants-1991_04 |
| ORD ID | ord-c8cfc1ea41c640a39693d56401eb3774 |
| 출처 메모 | uspto-grants-1991_04 |