Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → Dimethyl 3-(1-naphthyl)-2-isoxazolin-5-ylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Chlorosuccinimide | HCID 31398 | — |
| 반응물 | Dimethyl vinylphosphonate | HCID 78376 | — |
| 반응물 | 1-Naphthalenecarboxaldehyde, oxime | HCID 240801 | — |
| 생성물 | Dimethyl 3-(1-naphthyl)-2-isoxazolin-5-ylphosphonate | HCID 20062404 | — |
반응 단계
Preparation is carried out in analogy to Example 1 from 31.2 g (0.2 mol) of 1-naphthaldoxime, 29.4 g (0.22 mol) of N-chlorosuccinimide, 29.2 ml (0.22 mol) of dimethyl vinylphosphonate and 30.6 ml (0.22 mol) of triethylamine, with 56 g of oily compound being obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05006515 |
| 출처 데이터셋 | uspto-grants-1991_04 |
| ORD ID | ord-c8375bb701b14142941725e3d7153d4e |
| 출처 메모 | uspto-grants-1991_04 |