Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenyl isocyanate → Methyl 3-benzyl-2-isoxazolin-5-yl(P-methyl)phosphinate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenyl isocyanate | HCID 7672 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 1-Nitro-2-phenylethane | HCID 80208 | — |
| 반응물 | Methyl methylvinylphosphinate | HCID 6454580 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | Methyl 3-benzyl-2-isoxazolin-5-yl(P-methyl)phosphinate | HCID 20062386 | 79% |
반응 단계
Preparation is carried out in analogy to Example 23 from 37.1 ml (0.34 mol) of phenyl isocyanate, 22.5 g (0.187 mol) of methyl vinyl(P-methyl)phosphinate, 4 ml of triethylamine and 25.7 g (0.17 mol) of 2-phenylnitroethane in toluene, resulting in 34 g of brown oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05006515 |
| 출처 데이터셋 | uspto-grants-1991_04 |
| ORD ID | ord-a078aed30ebf450481812bf743e1fd6f |
| 출처 메모 | uspto-grants-1991_04 |