Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → Diethyl 3-tert.butyl-2-isoxazolin-5-ylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Chlorosuccinimide | HCID 31398 | — |
| 반응물 | Diethyl vinylphosphonate | HCID 69629 | — |
| 반응물 | Pivalaldoxime | HCID 136457 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Diethyl 3-tert.butyl-2-isoxazolin-5-ylphosphonate | HCID 86744708 | — |
반응 단계
The procedure is analogous to that of Example 25 using 15.2 g (0.15 mol) of pivalaldoxime, 22.0 g (0.165 mol) of N-chlorosuccinimide, 0.5 ml of pyridine, 27.1 g (0.165 mol) of diethyl vinylphosphonate and 22.9 ml (0.165 mol) of triethylamine in dichloromethane. The product is obtained as an oil after the usual working up.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05006515 |
| 출처 데이터셋 | uspto-grants-1991_04 |
| ORD ID | ord-f7ff29b72e2e4375b1d0bcfc664d7b01 |
| 출처 메모 | uspto-grants-1991_04 |