Methylamine → HCID 13983506, 화합물

HRID 1084924노트

반응식

HRID 1084924 반응식
[CH3:1][NH2:2].Cl[S:4]([C:7]1[CH:8]=[C:9]2[C:14](=[C:15]([C:17]([OH:19])=[O:18])[CH:16]=1)[O:13][CH2:12][CH2:11][CH2:10]2)(=[O:6])=[O:5]>>[CH3:1][NH:2][S:4]([C:7]1[CH:8]=[C:9]2[C:14](=[C:15]([C:17]([OH:19])=[O:18])[CH:16]=1)[O:13][CH2:12][CH2:11][CH2:10]2)(=[O:6])=[O:5]

참가 물질

3

반응물 2

HCID 6329MethylamineHCID 20062876HCID 20062876, 화합물

생성물 1

HCID 13983506HCID 13983506, 화합물

실험 절차

207 g of a 40% aqueous solution of methylamine were introduced into a 1-liter round-bottomed flask and 123 g of finely ground 6-chlorosulphonylchroman-8-carboxylic acid were then added in portions, while maintaining the temperature between 0° C. and 5° C., by cooling.

후처리

  1. temperaturewhile maintaining the temperature between 0° C. and 5° C.
  2. temperatureby cooling

출처 및 근거

ORD 기록
ord-8a9a6f240dda414e9914ff9743b4b785
출처 데이터셋
uspto-grants-1991_04
특허 번호
US05006570

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