Potassium Carbonate → HCID 19826066, 화합물

HRID 1085052노트

반응식

HRID 1085052 반응식
Cl.[F:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][NH2:11])=[CH:5][CH:4]=1.C([O-])([O-])=O.[K+].[K+].[Cl:18][CH2:19][CH2:20][CH2:21][C:22]1[C:26]2[CH:27]=[C:28]([O:33][CH3:34])[C:29]([O:31][CH3:32])=[CH:30][C:25]=2[O:24][N:23]=1>CN(C=O)C>[ClH:18].[F:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][NH:11][CH2:19][CH2:20][CH2:21][C:22]2[C:26]3[CH:27]=[C:28]([O:33][CH3:34])[C:29]([O:31][CH3:32])=[CH:30][C:25]=3[O:24][N:23]=2)=[CH:5][CH:4]=1

참가 물질

5

반응물 3

HCID 11430Potassium CarbonateHCID 197725Phenethylamine, p-fluoro-, hydrochlorideHCID 14837050HCID 14837050, 화합물

생성물 1

HCID 19826066HCID 19826066, 화합물

시약·촉매·용매 1

HCID 6228Dimethylformamide용매

실험 절차

To 100 ml of dry DMF were added 2-(4-fluorophenyl)-ethylamine hydrochloride (10 g) and milled K2CO3 (20 g). After five minutes of stirring, 3-(3-chloropropyl)-5,6-dimethoxy-1,2-benzisoxazole (6.4 g) and KI (0.01 g) were added.

출처 및 근거

ORD 기록
ord-a9f7bb4365e74f6194ba0412423b3803
출처 데이터셋
uspto-grants-1991_04
특허 번호
US05008264

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