Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl hydroperoxide → t-Amylperoxy 2,4-dimethylphenyl carbonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl hydroperoxide | HCID 6410 | — |
| 반응물 | Phenyl chloroformate | HCID 15891 | — |
| 반응물 | tert-Amyl hydroperoxide | HCID 76962 | — |
| 반응물 | 2,4-Dimethylphenyl chloroformate | HCID 15917593 | — |
| 생성물 | t-Amylperoxy 2,4-dimethylphenyl carbonate | HCID 54014625 | 65% |
반응 단계
A reaction was carried out in the same manner as described in Example 1, except that t-amyl hydroperoxide and 2,4-dimethylphenyl chloroformate were used in place of t-butyl hydroperoxide and phenyl chloroformate used in Example 1, to obtain 35.7 g (yield: 65%) of a compound having a GLC purity of 92%, which was a colorless liquid at room temperature.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05008353 |
| 출처 데이터셋 | uspto-grants-1991_04 |
| ORD ID | ord-5d97dd5a689543be805316febca72878 |
| 출처 메모 | uspto-grants-1991_04 |