1,3-Dibromopropane → 1-Bromo-3-[3-(octadecyloxy)propoxy]propane

HRID 1085378

반응식

HRID 1085378 반응식
[CH2:1]([O:19][CH2:20][CH2:21][CH2:22][OH:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[Br:24][CH2:25][CH2:26][CH2:27]Br>[Cl-].C([N+](C)(C)C)CCCCCCCCCCCCCCC>[Br:24][CH2:25][CH2:26][CH2:27][O:23][CH2:22][CH2:21][CH2:20][O:19][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

참가 물질

4

반응물 2

HCID 80011,3-DibromopropaneHCID 5553033-Octadecyloxypropanol

생성물 1

HCID 200621421-Bromo-3-[3-(octadecyloxy)propoxy]propane수율 7.7%

시약·촉매·용매 1

HCID 8154Hexadecyltrimethylammonium chloride촉매

실험 절차

Employing 3-(octadecyloxy)propanol (5 g), 1,3-dibromopropane (9.2 g) and cetyltrimethylammonium chloride (0.97 g), a reaction and aftertreatment are conducted in the same manner as those in Reference Example 4 to obtain the above-titled compound (0.53 g).

출처 및 근거

ORD 기록
ord-9a0d23e8c49345a0b3ac1efca027cd60
출처 데이터셋
uspto-grants-1991_04
특허 번호
US05008454

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