Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5'-fluoro-N-methyl-2'-methylsulphinylacetylformanilide → Flosequinan
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5'-fluoro-N-methyl-2'-methylsulphinylacetylformanilide | HCID 86744741 | — |
| 용매 | 2-Methoxyethanol | HCID 8019 | — |
| 생성물 | Flosequinan | HCID 4474062 | — |
반응 단계
A solution of 5'-fluoro-N-methyl-2'-methylsulphinylacetylformanilide (0.77 g) in 2-methoxyethanol (25 ml) was heated to reflux over 20 minutes. After heating under reflux at 128° for 45 minutes the mixture was evaporated in vacuo to give 7-fluoro-1-methyl-3-methylsulphinyl-4-quinolone, m.p.225.5°-227° (0.69 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05011931 |
| 출처 데이터셋 | uspto-grants-1991_04 |
| ORD ID | ord-6d07a6becd3e4270be25d4f2c5fdfd93 |
| 출처 메모 | uspto-grants-1991_04 |