Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Quinoxalin-6-ylmethanol → Quinoxaline-6-carboxaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Quinoxalin-6-ylmethanol | HCID 6422829 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Quinoxaline-6-carboxaldehyde | HCID 763958 | 67.3% |
반응 단계
To a stirred solution of 10 parts of intermediate 5, namely 6-quinoxalinemethanol in 133 parts of dichloromethane were added 20 parts of manganese(IV) oxide. After stirring for 3 hours at room temperature, the reaction mixture was filtered and the filtrate was evaporated, yielding 6.6 parts (67.3%) of 6-quinoxalinecarboxaldehyde; mp. 134° C. (interm. 6).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05028606 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-65c5ab1fe71e481b8c78200566367692 |
| 출처 메모 | uspto-grants-1991_07 |