Tartrate → Tartrate maleate

HRID 1086317

반응식

HRID 1086317 반응식
[Ca].[C:2]([C@@H:5]([C@H:7]([C:9]([O-:11])=[O:10])[OH:8])[OH:6])([O-:4])=[O:3].[C:12]([O-:19])(=[O:18])/[CH:13]=[CH:14]\[C:15]([OH:17])=[O:16].[Na+]>>[C:2]([CH:5]([CH:7]([C:9]([O-:11])=[O:10])[OH:8])[OH:6])([O-:4])=[O:3].[C:12]([O-:19])(=[O:18])/[CH:13]=[CH:14]\[C:15]([O-:17])=[O:16]

참가 물질

4

실험 절차

In the production of HOPTC and DOOHC it is preferred that calcium D, L-tartrate and monosodium maleate slurry obtained from the tartrate/maleate removal step is added to the calcium maleate while heating to a boil at atmospheric pressure. The mixture is held at boiling for about 15 minutes to ensure conversion of all of the calcium carbonate to the maleate. The mixture is then charged to the synthesis reactor for the preparation of additional HOPTC and DOOHC. During transfer to the synthesis reactor water may be evaporated to reduce volume.

출처 및 근거

ORD 기록
ord-38ec9c37b90f45dca9a8e67f1d7bbc67
출처 데이터셋
uspto-grants-1991_07
특허 번호
US05028723

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