Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanolamine → 2-Pentyl-2-oxazoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanolamine | HCID 700 | — |
| 반응물 | Hexanenitrile | HCID 12352 | — |
| 반응물 | Dodecanenitrile | HCID 17092 | — |
| 촉매 | Zinc acetate (USP) | HCID 2724192 | — |
| 생성물 | 2-Pentyl-2-oxazoline | HCID 14651790 | 60% |
반응 단계
9.72 g (100 mmoles) of hexanenitrile was substituted for undecyl cyanide in Example 1 and the reaction was repeated with 6.11 g (100 mmoles) of ethanolamine and 549 mg (2.5 mmoles) of zinc acetate dihydrate under identical conditions. At the end of the reaction the product was worked up as before and distilled at 73° C./10 mm to give 8.2 g (60%) of 2-pentyl-2-oxazoline.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05030629 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-5dac6adbfadc472fa1136602ebb1d453 |
| 출처 메모 | uspto-grants-1991_07 |