Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Aminopropanol → 4-Methyl-2-undecyl-2-oxazoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Aminopropanol | HCID 5126 | — |
| 반응물 | Dodecanenitrile | HCID 17092 | — |
| 촉매 | Cadmium acetate, dihydrate | HCID 6537495 | — |
| 용매 | 1-Butanol | HCID 263 | — |
| 생성물 | 4-Methyl-2-undecyl-2-oxazoline | HCID 14651791 | 92% |
반응 단계
10.9 g (60 mmoles) of undecyl cyanide was treated with 5 g (66.6 mmoles) of DL-2-amino-1-propanol in presence of 400 mg (1.5 mmoles) of cadmium acetate dihydrate in 1-butanol as outlined under Example 1. 13.2 g (92%) of product was obtained on distillation at 115°-117° C./1-1.5 mm Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05030629 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-8fcaecc793d94a60abd145079f17f86a |
| 출처 메모 | uspto-grants-1991_07 |