Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dodecanenitrile → 4-Ethyl-2-undecyl-2-oxazoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dodecanenitrile | HCID 17092 | — |
| 반응물 | 2-Amino-1-butanol | HCID 22129 | — |
| 촉매 | Cadmium acetate, dihydrate | HCID 6537495 | — |
| 용매 | 1-Butanol | HCID 263 | — |
| 생성물 | 4-Ethyl-2-undecyl-2-oxazoline | HCID 226848 | 89.6% |
반응 단계
25 g (137.9 mmoles) of undecyl cyanide was treated with 15.2 ml (165 mmoles) of DL-2-amino-1-butanol in presence of 919 mg (3.54 mmoles) of cadmium acetate dihydrate in 1-butanol as outlined under Example 1. 31.31 g (89.6%) of product was obtained on distillation at 124°-125° C./1.2-1.4 mm Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05030629 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-8914f7dabadf434ab6e49ee2880f2582 |
| 출처 메모 | uspto-grants-1991_07 |