Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexanenitrile → HCID 178442284, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexanenitrile | HCID 12352 | — |
| 반응물 | 2-Methylpropylenediamine | HCID 13128 | — |
| 용매 | Carbon Disulfide | HCID 6348 | — |
| 생성물 | HCID 178442284 | HCID 178442284 | 73.4% |
반응 단계
8.41 g (95.4 mmoles) of 1,2-diamino-2-methylpropane, 7.4 g (76.16 mmoles) of hexanenitrile and 0.4 ml of carbon disulfide were heated at 125° C. for 24 hours and then worked up as under Example 23. Distillation at 105°-107° C./0.5 mm gave 9.4 g (73.4%) of product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05030629 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-774414b09cb54582b80ce98d82d5fa71 |
| 출처 메모 | uspto-grants-1991_07 |