2-Amino-3-methoxybenzamide → HCID 19826361, 화합물

반응식

[CH3:1][O:2][C:3]1[CH:11]=[CH:10][CH:9]=[C:5]([C:6]([NH2:8])=[O:7])[C:4]=1[NH2:12].Br[C:14]1[S:15][C:16]([Br:20])=[C:17]([CH3:19])N=1>>[Br:20][C:16]1[S:15][C:14]2=[N:12][C:4]3[C:5]([C:6](=[O:7])[N:8]2[C:17]=1[CH3:19])=[CH:9][CH:10]=[CH:11][C:3]=3[O:2][CH3:1]

참가 물질

반응물 2

HCID 185365712-Amino-3-methoxybenzamide

HCID 220564022,5-Dibromo-4-methyl-1,3-thiazole

생성물 1

HCID 19826361HCID 19826361, 화합물수율 77.7%

실험 절차

4.8 g of 3-methoxyanthranilamide and 7.5 g of 2,5-dibromo-4-methylthiazole were stirred for 12 hours at 140° C. After working up in the conventional manner there was obtained 7.3 g (77%) of the above compound; m.p. 198°-199° C.

출처 및 근거

ORD 기록: ord-560d2370e0d64241912bda0c53975f1a
출처 데이터셋: uspto-grants-1991_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05030727

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