Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Octyloxy)benzoic acid | HCID 17231 | — |
| 반응물 | Phosphorus pentachloride | HCID 24819 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 4-Octyloxybenzoyl chloride | HCID 2760250 | — |
반응 단계
2.78 g of 4-octyloxybenzoic acid was added to 10 ml of benzene, and under stirring at room temperature, 2.36 g of PCl5 was added little by little. The mixture was then heated under reflux for 4 hours. Thereafter, the solvent was distilled off to obtain 4-octyloxybenzoic acid chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05034152 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-d0c650b3ad4245688f41bd261bc78567 |
| 출처 메모 | uspto-grants-1991_07 |