Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chloromethyl hexanoate → HCID 178445524, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chloromethyl hexanoate | HCID 525229 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 반응물 | HCID 178527738 | HCID 178527738 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | HCID 178445524 | HCID 178445524 | — |
반응 단계
23.1 g hexanoic acid chloromethyl ester are added over a period of 30 minutes with stirring to 17.2 g 4-mercapto-1,2,3-triazole, sodium salt, in 100 ml dimethyl formamide. After 2 h, the mixture is added to 600 ml ice water and the oil formed is taken up in ethyl acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05035987 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-e85c571e73c74af58ee5112d07b27c71 |
| 출처 메모 | uspto-grants-1991_07 |