Chloromethyl hexanoate → HCID 178445524, 화합물

HRID 1087367

반응식

HRID 1087367 반응식
Cl[CH2:2][O:3][C:4](=[O:10])[CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].[SH:11][C:12]1[N:13]=[N:14][NH:15][CH:16]=1.[Na]>CN(C)C=O.C(OCC)(=O)C>[CH2:5]([C:4]([O:3][CH2:2][S:11][C:12]1[N:13]=[N:14][NH:15][CH:16]=1)=[O:10])[CH2:6][CH2:7][CH2:8][CH3:9]

참가 물질

6

반응물 3

HCID 525229Chloromethyl hexanoateHCID 5360545SodiumHCID 178527738HCID 178527738, 화합물

생성물 1

HCID 178445524HCID 178445524, 화합물

시약·촉매·용매 2

HCID 6228Dimethylformamide용매HCID 8857Ethyl Acetate용매

실험 절차

23.1 g hexanoic acid chloromethyl ester are added over a period of 30 minutes with stirring to 17.2 g 4-mercapto-1,2,3-triazole, sodium salt, in 100 ml dimethyl formamide. After 2 h, the mixture is added to 600 ml ice water and the oil formed is taken up in ethyl acetate.

후처리

  1. customthe oil formed

출처 및 근거

ORD 기록
ord-e85c571e73c74af58ee5112d07b27c71
출처 데이터셋
uspto-grants-1991_07
특허 번호
US05035987

연결된 노트

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