Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Epichlorohydrin → 3-(2-Benzyl-4-chlorophenoxy)-1,2-epoxypropane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Epichlorohydrin | HCID 7835 | — |
| 반응물 | Chlorophene | HCID 8425 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | 3-(2-Benzyl-4-chlorophenoxy)-1,2-epoxypropane | HCID 14369940 | — |
반응 단계
A suspension containing 21.87 g of 2-benzyl-4-chlorophenol, 27.76 g of 1-chloro-2,3-epoxypropane and 27.64 g of potassium carbonate in 200 ml of butanone is refluxed for 12 hours. The inorganic salts formed are filtered off and drained. The solvent and excess 1-chloro-2,3-epoxypropane are evaporated off under vacuum and the residue is distilled at between 160° C. and 180° C. under 0.01 mm of mercury.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05036077 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-f9f619d136424341bc05c2fa1bf5aa73 |
| 출처 메모 | uspto-grants-1991_07 |