Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Epichlorohydrin → 3-(1-Bromonaphth-2-yloxy)-1,2-epoxypropane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Epichlorohydrin | HCID 7835 | — |
| 반응물 | 1-Bromo-2-naphthol | HCID 11316 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | 3-(1-Bromonaphth-2-yloxy)-1,2-epoxypropane | HCID 14369942 | — |
반응 단계
A suspension containing 22.3 g of 1-bromonaphth-2-ol, 27.75 g of 1-chloro-2,3-epoxypropane and 27.6 g of potassium carbonate in 200 ml of butanone is refluxed overnight. The inorganic salts are filtered off and drained and the filtrate is then evaporated under vacuum. The oil obtained is distilled under 0.01 mm of mercury.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05036077 |
| 출처 데이터셋 | uspto-grants-1991_07 |
| ORD ID | ord-e743b44489f04654891d9a3d50b33511 |
| 출처 메모 | uspto-grants-1991_07 |