1,2-Bis(2-chloroethoxy)ethane → 1,8-Bis[(2-pyridyl)(phenyl)phosphino]-3,6-dioxaoctane

HRID 1087712

반응식

HRID 1087712 반응식
N1C=CC=CC=1P([CH2:14][P:15]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][N:17]=1)C1C=CC=CC=1.ClC[CH2:30][O:31][CH2:32][CH2:33][O:34][CH2:35][CH2:36]Cl>ClCCl>[N:17]1[CH:18]=[CH:19][CH:20]=[CH:21][C:16]=1[P:15]([C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1)[CH2:36][CH2:35][O:34][CH2:33][CH2:32][O:31][CH2:30][CH2:14][P:15]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][N:17]=1)[C:22]1[CH:23]=[CH:24][CH:25]=[CH:26][CH:27]=1

참가 물질

4

반응물 2

HCID 81711,2-Bis(2-chloroethoxy)ethaneHCID 22163400Bis[(2-pyridyl)(phenyl)phosphino]methane

생성물 1

HCID 198031491,8-Bis[(2-pyridyl)(phenyl)phosphino]-3,6-dioxaoctane

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

Some 1,8-bis[(2-pyridyl)(phenyl)phosphino]-3,6-dioxaoctane was prepared substantially in the same way as the diphosphine of Example 2, except that instead of dichloromethane, 1,8-dichloro-3,6-dioxaoctane was employed.

출처 및 근거

ORD 기록
ord-d21844c117974186a1ceb2d96539f74a
출처 데이터셋
uspto-grants-1990_10
특허 번호
US04960747

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