Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Epichlorohydrin → 1-Benzenesulfonyl-4-(3-chloro-2-hydroxypropyl)piperazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Epichlorohydrin | HCID 7835 | — |
| 반응물 | 1-(Benzenesulfonyl)piperazine | HCID 808712 | — |
| 생성물 | 1-Benzenesulfonyl-4-(3-chloro-2-hydroxypropyl)piperazine | HCID 14719872 | 98.7% |
반응 단계
Epichlorohydrin (0.5 g) and 3.7 g of 1-benzenesulfonylpiperazine were reacted and worked up in the same way as in Referential Example 1 to give 1.7 g of 1-benzenesulfonyl-4-(3-chloro-2-hydroxypropyl)piperazine as a colorless powdery crystal having a melting point of 136 to 137° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04960883 |
| 출처 데이터셋 | uspto-grants-1990_10 |
| ORD ID | ord-ba92a102c7c44ba78f34d2ae55fffc90 |
| 출처 메모 | uspto-grants-1990_10 |