참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,4-Butanediol | HCID 8064 | — |
| 반응물 | Octacosanoic acid | HCID 10470 | — |
| 반응물 | Tin atom | HCID 5352426 | — |
| 생성물 | 1,4-Butanediol monomontanate | HCID 17977842 | — |
반응 단계
57.2 g 1,4-butanediol (0.636 mole), 254.2 g montanic acid and 0.4 g tin powder were heated to 210° C. as in Example 1 with application of a gentle vacuum. The vacuum was increased to 152 mbar over a period of 3 hours. The mixture had an acid value of 1.5. A brownish-yellow wax having a dropping point of 77° C. was obtained after cooling to 100° C., bleaching and filtering.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04962145 |
|---|
| 출처 데이터셋 | uspto-grants-1990_10 |
|---|
| ORD ID | ord-ea9cfb6e2aaf48e99c51445608d5ceb9 |
|---|
| 출처 메모 | uspto-grants-1990_10 |
|---|
