참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Sorbitol | HCID 5780 | — |
| 반응물 | Octacosanoic acid | HCID 10470 | — |
| 반응물 | Tin atom | HCID 5352426 | — |
| 생성물 | Sorbitol trimontanate | HCID 86744265 | — |
반응 단계
41.1 g sorbitol (0.226 mole), 271.1 g montanic acid (0.678 mole) and 0.4 g tin powder were heated to 200° C. as in Example 1 with application of a gentle vacuum. The vacuum was increased to 15 mbar over a period of 14 h, by which time the acid value had fallen to 5. After cooling to 100° C., the product was filtered, giving a brown hard wax having a dropping point of 78° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US04962145 |
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| 출처 데이터셋 | uspto-grants-1990_10 |
|---|
| ORD ID | ord-ad12c830b0954be2b0ad1e72ee90f6ba |
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| 출처 메모 | uspto-grants-1990_10 |
|---|