Benzene → Benzenamine, 4-methoxy-N-(1-phenylethylidene)-
반응식
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=O)[CH3:2].[CH3:10][O:11][C:12]1[CH:17]=[CH:16][C:15]([NH2:18])=[CH:14][CH:13]=1.C1C=CC=CC=1>O>[CH3:2][C:1](=[N:18][C:15]1[CH:16]=[CH:17][C:12]([O:11][CH3:10])=[CH:13][CH:14]=1)[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1참가 물질
5
실험 절차
A solution of acetophenone (64 ml), p-anisidine (65 mg), benzene (100 ml) was refluxed in the presence of molecular sieve (100 g) with continuous removal of water. The crude product was purified by crystallizing it from ethanol to give N-(αmethyl-benzylidene)-p-anisidine (VII) (50 g). VII had a melting point of 81°-82° C.
후처리
- customThe crude product was purified
- customby crystallizing it from ethanol
출처 및 근거
- ORD 기록
- ord-2a2fc40be80a4e3baeb746a53558c36c
- 출처 데이터셋
- uspto-grants-1990_10
- 특허 번호
- US04962234
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