Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3',4',5'-Trimethoxyacetophenone → 3-(4-Hydroxy-3-methoxy-5-nitrophenyl)-1-(3,4,5-trimethoxyphenyl)prop-2-en-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3',4',5'-Trimethoxyacetophenone | HCID 14345 | — |
| 반응물 | 5-Nitrovanillin | HCID 81134 | — |
| 생성물 | 3-(4-Hydroxy-3-methoxy-5-nitrophenyl)-1-(3,4,5-trimethoxyphenyl)prop-2-en-1-one | HCID 3430178 | — |
반응 단계
The procedure described in Example 8 was repeated by using 2.0 g of 4-hydroxy-3-methoxy-5-nitrobenzaldehyde and 2.1 g of 3',4',5'-trimethoxyacetophenone. Yield 2.2 g (57%), m.p. 123°-125° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04963590 |
| 출처 데이터셋 | uspto-grants-1990_10 |
| ORD ID | ord-7d132b4db3dd4449976bf79c4d9d3b60 |
| 출처 메모 | uspto-grants-1990_10 |