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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1089037생성일: 2026년 10월 27일

Resorcinol → 1,3-Benzenediol, o-octanoyl-

https://huagongshe.com/reaction/1089037

반응식

참여 물질

역할이름HCID투입량
반응물ResorcinolHCID 5054—
반응물Octanoic anhydrideHCID 69340—
반응물Hydroquinone mono-acetateHCID 21327627—
반응물Octanoyloxy-3-hydroxy benzene (resorcinol monooctanoate)HCID 131716678—
촉매4-(Dimethylamino)pyridineHCID 14284—
용매TriethylamineHCID 8471—
용매Ethyl AcetateHCID 8857—
생성물1,3-Benzenediol, o-octanoyl-HCID 14549096—

반응 단계

Adapting the method of synthesis disclosed in D. Johnston, "Preparation of Hydroquinone Monoacetate," Chemistry & Industry 24:1000 (1982) (which is incorporated herein by reference), it is expected that resorcinol may be combined with about an equimolar amount of dioctanoic acid anhydride, and ethyl acetate solvent, a non-nucleophilic solvent, in the presence of 4-dimethylaminopyridine, a catalyst, and a base, such as triethylamine, at room temperature, to produce the desired 1 octanoyloxy-3-hydroxy benzene (resorcinol monooctanoate).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04964870
출처 데이터셋uspto-grants-1990_10
ORD IDord-6ce8d7de2557459fa3c9e28bf34037b6
출처 메모uspto-grants-1990_10