Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Thiopheneacetic acid → (2-Methanesulphonyl-1-ethylthio)tri-n-butyltin
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Thiopheneacetic acid | HCID 15970 | — |
| 반응물 | Methyl vinyl sulfone | HCID 19354 | — |
| 반응물 | TIN OXIDE (SnO) | HCID 88989 | — |
| 반응물 | (3-Oxo-1-butylthio)tri-n-butyltin | HCID 22158982 | — |
| 생성물 | (2-Methanesulphonyl-1-ethylthio)tri-n-butyltin | HCID 85601524 | 41% |
반응 단계
This compound was prepared analogously to (5), starting from thiolacetic acid and methylvinylsulphone, leading to the intermediate sulphone (47%), treating subsequently with the tin oxide to give the required product (6) (41%). All spectroscopic and analytical data were consistent with the proposed structures.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04966678 |
| 출처 데이터셋 | uspto-grants-1990_10 |
| ORD ID | ord-84bf2250030340d198919eefa26abb58 |
| 출처 메모 | uspto-grants-1990_10 |