HCID 14536735, 화합물 → HCID 14536738, 화합물

HRID 1089430노트

반응식

HRID 1089430 반응식
[C:1]([NH:4][CH2:5][CH2:6][N:7]1[C:11]([CH3:12])=[CH:10][C:9]([C:13]([O:15]CC2C=CC=CC=2)=[O:14])=[C:8]1[CH3:23])(=[O:3])[CH3:2]>C(O)C>[C:1]([NH:4][CH2:5][CH2:6][N:7]1[C:11]([CH3:12])=[CH:10][C:9]([C:13]([OH:15])=[O:14])=[C:8]1[CH3:23])(=[O:3])[CH3:2]

참가 물질

3

반응물 1

HCID 14536735HCID 14536735, 화합물

생성물 1

HCID 14536738HCID 14536738, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

2.4 g (7.6 mmol) of benzyl 1-(2-acetylaminoethyl)-2,5-dimethylpyrrole-3-carboxylate from Example 3 are dissolved in 200 ml of ethanol and hydrogenated in the presence of 0.5 g of 10% strength Pd-on-charcoal at room temperature. After the mixture has been concentrated, the resulting solid is stirred with methylene chloride and filtered off with suction.

후처리

  1. concentrationAfter the mixture has been concentrated
  2. filtrationfiltered off with suction

출처 및 근거

ORD 기록
ord-14d30af93e8f4ac49fafe16204dfe1e9
출처 데이터셋
uspto-grants-1990_10
특허 번호
US04966901

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