Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitromethane → 1-Methylthio-1-methylamino-2-nitroethylene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitromethane | HCID 6375 | — |
| 반응물 | N-Methyl-dithiocarbonimidic acid dimethyl ester | HCID 140427 | — |
| 생성물 | 1-Methylthio-1-methylamino-2-nitroethylene | HCID 123549 | — |
반응 단계
A mixture of nitromethane (3 ml), methyl carbonimidodithioic acid dimethyl ester (X, 675 mg), rare earth exchange Y-zeolite (RE 70 Na Y) (675 mg) was heated at 90°-110° C. for 72 hr. It was filtered and the solvent was removed by distillation leaving the required 1-methylamino-1-methylthio-2-nitroethene (II) as residue. m.p. 112°-114° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04967007 |
| 출처 데이터셋 | uspto-grants-1990_10 |
| ORD ID | ord-6ecac4db049f41c5b37fd8868d372dad |
| 출처 메모 | uspto-grants-1990_10 |