Thionyl Chloride → Monopropyl Terephthaloyl Chloride

HRID 1089643노트

반응식

HRID 1089643 반응식
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].[C:14](OCCC)(=O)[C:15]1C=CC(C([O-])=O)=CC=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:14][CH3:15]

참가 물질

5

반응물 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046, 화합물HCID 23693908Potassium Monopropyl Terephthalate

생성물 1

HCID 19915522Monopropyl Terephthaloyl Chloride

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

This compound was prepared by the procedure described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monopropyl terephthalate (49.0g, 0.20 mole), thionyl chloride (29.8g, 0.25 mole) and 100 ml of toluene. The product was used without further purification.

후처리

  1. customThis compound was prepared by the procedure
  2. customThe product was used without further purification

출처 및 근거

ORD 기록
ord-ac7eb9e4db084883b32afbccc60fb5aa
출처 데이터셋
uspto-grants-1992_01
특허 번호
US05078907

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