Thionyl Chloride → HCID 19915516, 화합물

HRID 1089646노트

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HRID 1089646 반응식
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].[C:14](OCCCC)(=O)[C:15]1C=CC(C([O-])=O)=C[CH:16]=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:14][CH2:15][CH3:16]

참가 물질

5

반응물 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046, 화합물HCID 23693905Potassium Monobutyl Terephthalate

생성물 1

HCID 19915516HCID 19915516, 화합물

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

This compound was prepared by the procedure described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monobutyl terephthalate (10.0 g, 0.0384 mole), thionyl chloride (4.57, 0.0384 mole) and 40 ml of toluene. The yield of product was 8.5 g (92%). This material was used without further purification.

후처리

  1. customThis compound was prepared by the procedure
  2. customThis material was used without further purification

출처 및 근거

ORD 기록
ord-93af8425e7774440b21e6142f5d1b490
출처 데이터셋
uspto-grants-1992_01
특허 번호
US05078907

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