Thionyl Chloride → Monohexyl Terephthaloyl Chloride

HRID 1089648노트

반응식

HRID 1089648 반응식
[CH3:1][C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5].C(OCCCCCC)(=O)[C:15]1[CH:23]=[CH:22]C(C([O-])=O)=[CH:17][CH:16]=1.[K+].S(Cl)(Cl)=O>C1(C)C=CC=CC=1>[CH2:1]([C:2]1[CH:10]=[C:9]([C:11]([Cl:13])=[O:12])[CH:8]=[CH:7][C:3]=1[C:4]([Cl:6])=[O:5])[CH2:17][CH2:16][CH2:15][CH2:23][CH3:22]

참가 물질

5

반응물 3

HCID 24386Thionyl ChlorideHCID 22057046HCID 22057046, 화합물HCID 23693907Potassium monohexyl terephthalate

생성물 1

HCID 19915510Monohexyl Terephthaloyl Chloride

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

This compound was prepared by the method described for monomethyl terephthaloyl chloride. Typical reagent levels were as follows: potassium monohexyl terephthalate (18.6 g, 0.64 mole), thionyl chloride (9.21 g, 0.774 mole) and 100 ml of toluene. The product was used without further purification.

후처리

  1. customThis compound was prepared by the method
  2. customThe product was used without further purification

출처 및 근거

ORD 기록
ord-5ebe672c30364d6da854725a7ce28276
출처 데이터셋
uspto-grants-1992_01
특허 번호
US05078907

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