Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Cyanide → 3-Benzyloxy-2-((2,6-dimethylpiperidino)amino)propionitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Cyanide | HCID 8929 | — |
| 반응물 | (Phenylmethoxy)acetaldehyde | HCID 108989 | — |
| 반응물 | 2,6-Dimethyl-1-piperidylamine | HCID 123482 | — |
| 생성물 | 3-Benzyloxy-2-((2,6-dimethylpiperidino)amino)propionitrile | HCID 19915656 | 81.2% |
반응 단계
12.8 g of 1-amino-2,6-dimethylpiperidine, 4.9 g of sodium cyanide and 15.0 g of benzyloxyacetaldehyde are reacted analogously to 8a). 23.3 g of 3-benzyloxy-2-((2,6-dimethylpiperidino)amino)propionitrile are obtained, which are employed in the following step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05079244 |
| 출처 데이터셋 | uspto-grants-1992_01 |
| ORD ID | ord-047c45d38cb140d885c8626a3ed8984d |
| 출처 메모 | uspto-grants-1992_01 |