Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methyl-3-nitrobenzyl alcohol → (3-Amino-2-methylphenyl)methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methyl-3-nitrobenzyl alcohol | HCID 90289 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | (3-Amino-2-methylphenyl)methanol | HCID 577175 | 101.4% |
반응 단계
A solution of 2-methyl-3-nitrobenzyl alcohol (2.0 g, 12 mmol) in ethanol (100 ml) was hydrogenated over 10% palladium/charcoal (0.1 g) for 2 hours, at an initial pressure of 3.5 bar. The solution was filtered through celite and evaporated to give 3-amino-2-methylbenzyl alcohol (1.67 g, quantitative), m.p. 104°-106°
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05082848 |
| 출처 데이터셋 | uspto-grants-1992_01 |
| ORD ID | ord-964ca6295eb64af1ac47407e4136b9c0 |
| 출처 메모 | uspto-grants-1992_01 |