Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Perfluorooctyl iodide → Methyl perfluorooctyl sulphide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Perfluorooctyl iodide | HCID 10491 | — |
| 반응물 | Dimethyl Disulfide | HCID 12232 | — |
| 반응물 | Sodium Phosphate, Dibasic | HCID 24203 | — |
| 반응물 | Sodium Dithionite | HCID 24489 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Methyl perfluorooctyl sulphide | HCID 10504381 | 20% |
반응 단계
Perfluorooctyl iodide (5.5 g), sodium dithionite (3 g), sodium hydrogen phosphate (3 g) and methyl disulphide (1 g) are stirred in dimethylformamide (10 cc) and water (5 cc) for 6 hours. After the usual treatment, methyl perfluorooctyl sulphide is obtained in 20% yield.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05082945 |
| 출처 데이터셋 | uspto-grants-1992_01 |
| ORD ID | ord-3d25a9144f3e4f1ea4e2f1fb5c981bc2 |
| 출처 메모 | uspto-grants-1992_01 |