2,3-Dimethylbenzaldehyde → N-(2,3-Dimethylbenzyl)cyclopropanamine

HRID 1092788

반응식

HRID 1092788 반응식
[CH3:1][C:2]1[C:9]([CH3:10])=[CH:8][CH:7]=[CH:6][C:3]=1[CH:4]=O.ClC1C(Cl)=CC=CC=1C[NH:15][CH:16]1[CH2:18][CH2:17]1>>[CH3:1][C:2]1[C:9]([CH3:10])=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][NH:15][CH:16]1[CH2:18][CH2:17]1

참가 물질

3

반응물 2

HCID 342242,3-DimethylbenzaldehydeHCID 834599Cyclopropyl-(2,3-dichloro-benzyl)-amine

생성물 1

HCID 43090146N-(2,3-Dimethylbenzyl)cyclopropanamine

실험 절차

1B was synthesized from 2,3-dimethylbenzaldehyde (5.0 g, 37.3 mmol) using the procedure described for 1A. Yield: 6.0 g (92%) as light yellow oil. ESI-MS:m/z 176.3 (M+H)+, HPLC retention time: T=1.340 min (FAST-2).

후처리

  1. customT=1.340 min (FAST-2)

출처 및 근거

ORD 기록
ord-b003401741a9406488afc3de131ceed5
출처 데이터셋
uspto-grants-2012_03
특허 번호
US08129538B1

연결된 노트

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