Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Nitroisophthalic acid → 4-Aminobenzene-1,3-dioic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Nitroisophthalic acid | HCID 3062438 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 4-Aminobenzene-1,3-dioic acid | HCID 11355852 | — |
반응 단계
To a solution of 4-nitro isophthalic acid (4 g, 18.95 mmol) in MeOH (200 mL) was added Pd/C (20%) and the mixture was hydrogenated at RT over night. The reaction mixture was filtered through Celite and filtrate concentrated under vacuum to give 4-amino isophthalic acid in 60% as a solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08133998B2 |
| 출처 데이터셋 | uspto-grants-2012_03 |
| ORD ID | ord-a70aad4b64f84b4ba0494f54b48628cb |
| 출처 메모 | uspto-grants-2012_03 |