참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Tetramethylammonium hydroxide | HCID 60966 | — |
| 반응물 | Phosphoric acid, bis(1,1-dimethylethyl) ester | HCID 429756 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | Tetramethylammonium ditert-butyl hydrogen phosphate | HCID 86609697 | — |
반응 단계
A solution of the di-tert-butyl hydrogen phosphate obtained in step a) was dissolved in acetone (10 ml) and cooled to 0° C. To this solution was added a 10% aqueous solution of tetramethylammonium hydroxide (2.4 ml, 2.6 mmol), and the homogeneous solution was evaporated under reduced pressure to provide a solid, which was crystallized from refluxing 1,2-dimethoxyethane to provide tetramethylammonium ditert-butyl hydrogen phosphate as a white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08143249B2 |
|---|
| 출처 데이터셋 | uspto-grants-2012_03 |
|---|
| ORD ID | ord-aaaa61214fe04edeb11468c485e4e1de |
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| 출처 메모 | uspto-grants-2012_03 |
|---|
