4,6-Dinitrobenzene-1,3-diamine → 1,2,4,5-Benzenetetraamine

HRID 1099504

반응식

HRID 1099504 반응식
[H][H].[NH2:3][C:4]1[C:9]([N+:10]([O-])=O)=[CH:8][C:7]([N+:13]([O-])=O)=[C:6]([NH2:16])[CH:5]=1>>[NH2:3][C:4]1[CH:5]=[C:6]([NH2:16])[C:7]([NH2:13])=[CH:8][C:9]=1[NH2:10]

참가 물질

3

반응물 2

HCID 2917964,6-Dinitrobenzene-1,3-diamineHCID 178418361HCID 178418361, 화합물

생성물 1

HCID 782611,2,4,5-Benzenetetraamine

실험 절차

contacting the reaction mixture formed in step (f) with hydrogen at a pressure in the range of about 0.31 to about 3.45 MPa and a temperature in the range of about 20° C. to about 100° C. to hydrogenate the 1,3-diamino-4,6-dinitrobenzene and produce 1,2,4,5-tetraminobenzene;

후처리

  1. customin the range of about 20° C. to about 100° C.

출처 및 근거

ORD 기록
ord-a42f5e53bfc34b31862368c003a020b3
출처 데이터셋
uspto-grants-2012_03
특허 번호
US08143450B1

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