Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Octylamine → N-Heptyl-N'-octylthiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Octylamine | HCID 8143 | — |
| 반응물 | Heptane, 1-isothiocyanato- | HCID 78152 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | N-Heptyl-N'-octylthiourea | HCID 12796254 | 105.2% |
반응 단계
To a solution of 3.14 grams (0.02 mole) n-heptylisothiocyanate dissolved in 15 milliliters of benzene is added 2.58 grams (0.02 mole) n-octylamine. The temperature rose to 41° C. The mixture was then refluxed on a steam-bath for about 20 minutes, until the mixture reached a neutral pH. The solution was then evaporated under vacuum. A yield of 6.03 grams of 1-n-heptyl-3-n-octylthiourea was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04310539 |
| 출처 데이터셋 | uspto-grants-1982_01 |
| ORD ID | ord-f2ffe0eb4f944759889d5de5e67aff59 |
| 출처 메모 | uspto-grants-1982_01 |