Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine → (3,4-diaMinophenyl)(Morpholino)Methanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine | HCID 9321 | — |
| 반응물 | Sodium borohydride | HCID 4311764 | — |
| 반응물 | 2-Nitro-4-morpholinocarbonylaniline | HCID 20553752 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | (3,4-diaMinophenyl)(Morpholino)Methanone | HCID 22411123 | — |
반응 단계
A solution of 0.14 g of ferrous sulfate heptahydrate in 15 ml of methanol is treated under nitrogen with 0.02 g of sodium borohydride. After 5 minutes, 2.5 g of 2-nitro-4-morpholinocarbonylaniline (as prepared in Example XXXIX) and 1 ml 64% hydrazine are added. The mixture is refluxed until reduction is complete (~4-6 hours) to afford 1,2-diamino-4-morpholinocarbonylbenzene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04312873 |
| 출처 데이터셋 | uspto-grants-1982_01 |
| ORD ID | ord-a334c2564d384db1ac4a3b280edab83a |
| 출처 메모 | uspto-grants-1982_01 |