참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-(Methylamino)ethanol | HCID 8016 | — |
| 반응물 | 1,2-Epoxyoctadecane | HCID 23872 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-2-Hydroxyethyl-N-2-hydroxyoctadecyl-N-methyl amine | HCID 19694636 | 67% |
반응 단계
A 300-ml flask equipped with a stirrer was charged with 26.85 g (0.1 mol) of 1,2-epoxyoctadecane, 7.51 g (0.1 mol) of N-methylethanolamine and 50 ml of ethanol, and the contents were stirred at 80° C. for 18 hours. After the solvent was distilled off under reduced pressure, the resultant residue was purified by column chromatography on silica gel, thereby obtaining 23.0 g (yield: 67%) of the title compound (IIc-2).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05723497 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-b816d25167cf4c2ca0b10e123324d743 |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
